Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloroform → 3-[4-(Hexadecylamino)benzoyl]-4-carboethoxythiazolidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloroform | HCID 6212 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Ethyl thiazolidine-4-carboxylate | HCID 103574 | — |
| 반응물 | 4-Hexadecylaminobenzoyl chloride hydrochloride | HCID 13255322 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 3-[4-(Hexadecylamino)benzoyl]-4-carboethoxythiazolidine | HCID 20437342 | — |
반응 단계
One-tenth mole of 4-(hexadecylamino)benzoyl chloride hydrochloride in methylene chloride is added to a solution of 0.1 mole of ethyl thiazolidine-4-carboxylate in chloroform containing two equivalents of triethylamine. After 5 hours at 20° C. the solution is filtered and evaporated to a white solid which is recrystallized from acetonitrile.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04136256 |
| 출처 데이터셋 | uspto-grants-1979_01 |
| ORD ID | ord-869c8e850a6c434ab05550bbed0b5235 |
| 출처 메모 | uspto-grants-1979_01 |