참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 4-(Chloromethyl)pyridinium chloride | HCID 74570 | — |
| 반응물 | N-(tert-butyl)benzohydrazide | HCID 1275961 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N'-t-butyl-N-isonicotinyl-N'-benzoylhydrazine | HCID 53730014 | — |
반응 단계
A solution of N'-t-butyl-N'-benzoylhydrazine (0.5 g, 0.00026 mol) in 10 ml of toluene was treated with 50% sodium hydroxide (0.6 g) followed by isonicotinyl chloride hydrochloride (0.47 g, 0.0026 mol). The mixture was stirred at 23° C. overnight. The solids were removed by filtration and washed with water followed by ether to afford N'-t-butyl-N-isonicotinyl-N'-benzoylhydrazine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05424333 |
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| 출처 데이터셋 | uspto-grants-1995_06 |
|---|
| ORD ID | ord-018de437086b4f2aafc2c6b42d5289d0 |
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| 출처 메모 | uspto-grants-1995_06 |
|---|
