2-[(Dodecyloxy)methyl]-1,4-bis(phenylmethyl)piperazine → HCID 19763547, 화합물

HRID 2165656노트

반응식

HRID 2165656 반응식
[CH2:1]([O:13][CH2:14][CH:15]1[CH2:20][N:19](CC2C=CC=CC=2)[CH2:18][CH2:17][N:16]1CC1C=CC=CC=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>C(O)C.O.[Pd]>[CH2:1]([O:13][CH2:14][CH:15]1[CH2:20][NH:19][CH2:18][CH2:17][NH:16]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

참가 물질

5

반응물 1

HCID 197635782-[(Dodecyloxy)methyl]-1,4-bis(phenylmethyl)piperazine

생성물 1

HCID 19763547HCID 19763547, 화합물

시약·촉매·용매 3

HCID 23938Palladium촉매HCID 702Ethanol용매HCID 962Water용매

실험 절차

An 8 g portion of the above piperazine in 130 ml of ethanol and 10 ml of water was hydrogenated with 10% palladium on carbon for 4 hours then filtered and the filtrate evaporated, giving 4.5 g of 2-[(dodecyloxy)methyl]piperazine.

후처리

  1. filtrationthen filtered
  2. customthe filtrate evaporated

출처 및 근거

ORD 기록
ord-37006b2f9666450aa9cec96aa77d59de
출처 데이터셋
uspto-grants-1990_07
특허 번호
US04940710

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