Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2166429생성일: 2026년 10월 26일
1,5-Pentanediol, 1,5-dimethanesulfonate → 1-Hexadecyloxy-3-[5-(methanesulfonyloxy)pentyloxy]-2-methylenepropane
https://huagongshe.com/reaction/2166429
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,5-Pentanediol, 1,5-dimethanesulfonate | HCID 16920 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 3-Hexadecyloxy-2-methylenepropan-1-ol | HCID 11358886 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 1-Hexadecyloxy-3-[5-(methanesulfonyloxy)pentyloxy]-2-methylenepropane | HCID 23039596 | — |
반응 단계
3-Hexadecyloxy-2-methylenepropan-1-ol (from Preparation 1) (4.45 g), sodium hydride dispersion (55-60% in oil, 1.4 g), and 1,5-dimethanesulfonyloxypentane (10.9 g) were mixed in dry dimethylformamide (33 ml) and stirred at 54° C. for 20 hours. Following the work-up procedure described in Preparation 7, the desired product was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04945098 |
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| 출처 데이터셋 | uspto-grants-1990_07 |
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| ORD ID | ord-c5158f21fbb643de986a729d7be71e49 |
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| 출처 메모 | uspto-grants-1990_07 |
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