Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N'-t-butyl-N'-(3-methylbenzoyl)hydrazine → N'-t-butyl-N-(2-phenyl-3-methylpentanoyl)-N'-(3-toluoyl)hydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N'-t-butyl-N'-(3-methylbenzoyl)hydrazine | HCID 15452040 | — |
| 반응물 | 3-Methyl-2-phenylvaleryl chloride | HCID 21886026 | — |
| 촉매 | Sodium Hydroxide | HCID 14798 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N'-t-butyl-N-(2-phenyl-3-methylpentanoyl)-N'-(3-toluoyl)hydrazine | HCID 15452019 | — |
반응 단계
To a stirred suspension of N'-t-butyl-N'-(3-toluoyl)hydrazine (0.7 g) in toluene (10 ml) and aqueous sodium hydroxide (12 drops of 50% aqueous sodium hydroxide) was added dropwise 2-phenyl-3-methyl-pentanoyl chloride (1.0 g). The reaction mixture was stirred overnight, diluted with hexanes and the solids filtered. The solids were washed with hexane and air dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05424333 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-40b8df1381f7498e92be0080b88467a1 |
| 출처 메모 | uspto-grants-1995_06 |