Ethanol hydrochloride → HCID 136351074, 화합물

반응식

[OH:1][C:2]1[C:9]([O:10][CH2:11][CH2:12][O:13][CH2:14][CH2:15][O:16][CH3:17])=[CH:8][CH:7]=[CH:6][C:3]=1[C:4]#[N:5].[CH3:18][CH2:19][OH:20].[ClH:21]>>[ClH:21].[OH:1][C:2]1[C:9]([O:10][CH2:11][CH2:12][O:13][CH2:14][CH2:15][O:16][CH3:17])=[CH:8][CH:7]=[CH:6][C:3]=1[C:4](=[NH:5])[O:20][CH2:19][CH3:18]

참가 물질

반응물 2

HCID 21887872Ethanol hydrochloride

HCID 58506482HCID 58506482, 화합물

생성물 1

HCID 136351074HCID 136351074, 화합물

실험 절차

A solution of 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzonitrile (6 g) in EtOH/HCl (g) (150 mL) was heated to 40° C. overnight in a sealed tube. The solvent was evaporated under vacuum and the residue (7 g, crude) was used for the next step without further purification.

후처리

customThe solvent was evaporated under vacuum
customthe residue (7 g, crude) was used for the next step without further purification

출처 및 근거

ORD 기록: ord-f4064b5af8634a8d83c77c9e1cbd28a0
출처 데이터셋: uspto-grants-2015_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09045440B2

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