1-(4-Chlorophenyl)cyclopentanecarbonitrile → 1-(4-Chlorophenyl)-cyclopentanecarbaldehyde

HRID 2169150노트

반응식

HRID 2169150 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2([C:13]#N)[CH2:12][CH2:11][CH2:10][CH2:9]2)=[CH:4][CH:3]=1.C1(C2(C=[O:27])CCCC2)C=CC=CC=1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2([CH:13]=[O:27])[CH2:12][CH2:11][CH2:10][CH2:9]2)=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 973841-(4-Chlorophenyl)cyclopentanecarbonitrileHCID 110951241-Phenylcyclopentane-1-carbaldehyde

생성물 1

HCID 214680001-(4-Chlorophenyl)-cyclopentanecarbaldehyde수율 98.23%

실험 절차

1-(4-chlorophenyl)-cyclopentanecarbaldehyde (22-02) (66 g, 98.23%) was synthesized from (4-chlorophenyl)-acetonitrile (21-02) (66 g, 321.95 mmol) as a white solid as a crude product following the procedure as described for 1-phenyl-cyclopentanecarbaldehyde (22-01).

출처 및 근거

ORD 기록
ord-30276e9de2ea4f52a9dd419dbfbcf9de
출처 데이터셋
uspto-grants-2015_06
특허 번호
US09045486B2

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