(1-Phenylcyclopentyl)methanol → 1-(p-Chlorophenyl)cyclopentanemethanol

HRID 2169152

반응식

HRID 2169152 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2([CH:13]=[O:14])[CH2:12][CH2:11][CH2:10][CH2:9]2)=[CH:4][CH:3]=1.C1(C2(CO)CCCC2)C=CC=CC=1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2([CH2:13][OH:14])[CH2:12][CH2:11][CH2:10][CH2:9]2)=[CH:6][CH:7]=1

참가 물질

3

반응물 2

HCID 123544(1-Phenylcyclopentyl)methanolHCID 214680001-(4-Chlorophenyl)-cyclopentanecarbaldehyde

생성물 1

HCID 27240171-(p-Chlorophenyl)cyclopentanemethanol수율 37.52%

실험 절차

[1-(4-chlorophenyl)-cyclopentyl]-methanol (23-02) (25 g, 37.52%) was synthesized from 1-(4-chlorophenyl)-cyclopentanecarbaldehyde (22-02) (66 g, 317.3 mmol) as a colourless liquid following the procedure as described for (1-phenyl-cyclopentyl)-methanol (23-01).

출처 및 근거

ORD 기록
ord-97402fbe3fad4caa8f7d8dbad8ea6da8
출처 데이터셋
uspto-grants-2015_06
특허 번호
US09045486B2

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