Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperonal → Bis(3,4-methylenedioxy)chalcone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperonal | HCID 8438 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Acetopiperone | HCID 76622 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Bis(3,4-methylenedioxy)chalcone | HCID 294346 | — |
반응 단계
A mixture of piperonal (460 mg) and 3,4-methylenedioxyacetophenone (500 mg) in ethanol (20 ml) was treated with 1M NaOH solution (4 ml), then the mixture was stirred overnight. The pale yellow crystalline solid was filtered off, washed with water then cold aqueous ethanol and dried to give pure bis(3,4-methylenedioxy)chalcone DC-0006B (476 mg, 53%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09051253B2 |
| 출처 데이터셋 | uspto-grants-2015_06 |
| ORD ID | ord-f07f4bc4c5814b05824736c9efcf4768 |
| 출처 메모 | uspto-grants-2015_06 |