Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Cyanopyridine → N-(pyridin-3-ylmethyl)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Cyanopyridine | HCID 79 | — |
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Rhodium | HCID 23948 | — |
| 생성물 | N-(pyridin-3-ylmethyl)aniline | HCID 1082702 | — |
반응 단계
A mixture of 3-cyanopyridine (10.4 g), aniline (101.8 g) and a 5% rhodium on carbon catalyst (1.0 g) was treated with hydrogen at 60 psig 30 deg C. for 13 hours in a rocking autoclave. The catalyst was removed by filtration and the filtrate analyzed by glc to show 3.7 g of N-phenyl-N-(3-pyridylmethyl)amine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05424436 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-2dc1b1df31414fdabba8d25b8bcdf139 |
| 출처 메모 | uspto-grants-1995_06 |