Methyl chloroformate → HCID 86701771, 화합물

HRID 2174127노트

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[C:1]([CH2:3][C:4]1[C:12]([O:13][CH3:14])=[CH:11][C:10]([CH3:15])=[C:9]2[C:5]=1[CH:6]=[CH:7][N:8]2[C:16]([O:18][C:19]([CH3:22])([CH3:21])[CH3:20])=[O:17])#[N:2].Cl[C:24]([O:26][CH3:27])=[O:25]>>[C:1]([CH:3]([C:4]1[C:12]([O:13][CH3:14])=[CH:11][C:10]([CH3:15])=[C:9]2[C:5]=1[CH:6]=[CH:7][N:8]2[C:16]([O:18][C:19]([CH3:22])([CH3:21])[CH3:20])=[O:17])[C:24]([O:26][CH3:27])=[O:25])#[N:2]

참가 물질

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HCID 6586Methyl chloroformate

HCID 86701770HCID 86701770, 화합물

생성물 1

HCID 86701771HCID 86701771, 화합물

실험 절차

The title compound was synthesized from tert-Butyl 4-(cyanomethyl)-5-methoxy-7-methyl-1H-indole-1-carboxylate (Example 155-B) using the same procedure as in Example 148-A using methyl chloroformate in the place of methyl bromoacetate. MS (ESI+) m/z 359.4 (M+H).

출처 및 근거

ORD 기록: ord-b0222a3639964be79d97dda9189d5a67
출처 데이터셋: uspto-grants-2015_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09056874B2

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