참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 6-Methyl-3-(2H-1,2,3-triazol-2-yl)picolinonitrile | HCID 68281582 | — |
| 생성물 | 6-methyl-3-(2H-1,2,3-triazol-2-yl)picolinic acid | HCID 59363733 | — |
반응 단계
To a solution of the title compound of Step A (730 mg, 4 mmol) in EtOH (10 mL) was added 4 N NaOH (1 mL, 4 mmol). The mixture was heated at 100° C. for 24 h. The reaction mixture was concentrated in vacuo to a white solid which was used without further purification in subsequent steps.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US09062078B2 |
|---|
| 출처 데이터셋 | uspto-grants-2015_06 |
|---|
| ORD ID | ord-eb837fd85db84ac6b61acf6793cc84d7 |
|---|
| 출처 메모 | uspto-grants-2015_06 |
|---|
