1-(2-bromoethyl)-2-methylbenzene → HCID 86640683, 화합물

반응식

[C:1]1([C:7]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[N:8][NH:9][C:10]2[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][CH:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:23][C:24]1[CH:32]=[CH:31][CH:30]=[CH:29][C:25]=1[CH2:26][CH2:27]Br>>[C:17]1([C:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)=[N:8][N:9]([CH2:27][CH2:26][C:25]2[CH:29]=[CH:30][CH:31]=[CH:32][C:24]=2[CH3:23])[C:10]2[CH:11]=[CH:12][C:13]([CH3:16])=[CH:14][CH:15]=2)[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

참가 물질

반응물 2

HCID 27569661-(2-bromoethyl)-2-methylbenzene

HCID 6426133HCID 6426133, 화합물

생성물 1

HCID 86640683HCID 86640683, 화합물

실험 절차

General procedure B was used to convert 1-(diphenylmethylene)-2-p-tolylhydrazine (200 mg, 0.69 mmol; Example 36A) and 2-methylphenethylbromide (278 mg, 1.4 mmol; Aldrich) to the title compound: MS (DCI/NH3) m/z 404 (M+H)+.

출처 및 근거

ORD 기록: ord-bfb327bc7ba84d44997b1727f553094e
출처 데이터셋: uspto-grants-2015_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09063126B2

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