Benzamide → HCID 21192648, 화합물

HRID 217730노트

반응식

HRID 217730 반응식
[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12])[C:5]([OH:7])=O.[C:15](N)(=O)C1C=CC=CC=1>>[Cl:1][C:2]1[CH:3]=[C:4]([C:5](=[O:7])[CH3:15])[CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12]

참가 물질

3

반응물 2

HCID 2331BenzamideHCID 2400533-Chloro-4,5-dimethoxybenzoic acid

생성물 1

HCID 21192648HCID 21192648, 화합물

실험 절차

3-Chloro-4,5-dimethoxybenzoic acid (1 g) was converted to the benzamide derivative analogously to O3.043, and the latter to the title compound analogously to O2.059. 495 mg of the title compound were obtained. LC-MS rt: 1.55 min [M+H]+: 215.1 (met. a)

출처 및 근거

ORD 기록
ord-7441587f7f4c4211a83df5f54d8fdd34
출처 데이터셋
uspto-grants-2012_06
특허 번호
US08198272B2

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