Thioguaiacol → HCID 67107546, 화합물

HRID 2177743노트

반응식

HRID 2177743 반응식
[Br:1][C:2]1[C:3]([O:21][CH3:22])=[C:4]([C:10]([CH2:13][S:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[CH:11][CH:12]=1)[C:5]([O:7][CH2:8]C)=[O:6].BrC1C(OC)=C(C(CBr)=CC=1)[C:27](OC)=[O:28].COC1C=CC=CC=1S>>[Br:1][C:2]1[C:3]([O:21][CH3:22])=[C:4]([C:10]([CH2:13][S:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=2[O:28][CH3:27])=[CH:11][CH:12]=1)[C:5]([O:7][CH3:8])=[O:6]

참가 물질

4

반응물 3

HCID 23642ThioguaiacolHCID 66685947Methyl 3-bromo-6-bromomethyl-2-methoxybenzoate2회HCID 67107500HCID 67107500, 화합물

생성물 1

HCID 67107546HCID 67107546, 화합물

실험 절차

Prepared by proceeding in a similar manner to Intermediate 73, starting from methyl 3-bromo-6-bromomethyl-2-methoxybenzoate (Intermediate 89) and 2-methoxythiophenol.

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-744cf19d88964f20acb4ebb932b0ffa4
출처 데이터셋
uspto-grants-2015_06
특허 번호
US09067905B2

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