3-Chlorothiophenol → HCID 67107689, 화합물

HRID 2177746노트

반응식

HRID 2177746 반응식
BrC1C(OC)=C(C=CC=1CSC1C=CC=CC=1C)C(OCC)=O.[Br:24][C:25]1[C:26]([O:44][CH3:45])=[C:27]([C:33]([CH2:36][S:37][C:38]2[CH:43]=[CH:42][CH:41]=[CH:40][CH:39]=2)=[CH:34][CH:35]=1)[C:28]([O:30][CH2:31][CH3:32])=[O:29].[Cl:46]C1C=C(S)C=CC=1>>[Br:24][C:25]1[C:26]([O:44][CH3:45])=[C:27]([C:33]([CH2:36][S:37][C:38]2[CH:43]=[CH:42][CH:41]=[C:40]([Cl:46])[CH:39]=2)=[CH:34][CH:35]=1)[C:28]([O:30][CH2:31][CH3:32])=[O:29]

참가 물질

4

반응물 3

HCID 162573-ChlorothiophenolHCID 67107500HCID 67107500, 화합물2회HCID 67107587Ethyl 3-bromo-2-methoxy-(2-methylphenylthiomethyl)benzoate

생성물 1

HCID 67107689HCID 67107689, 화합물

실험 절차

Prepared by proceeding in a similar manner to Intermediate 77, starting from ethyl 3-bromo-6-bromomethyl-2-methoxybenzoate (Intermediate 87) and 3-chlorothiophenol.

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-1adf9c0e73ee43fabe11ffbc7093b714
출처 데이터셋
uspto-grants-2015_06
특허 번호
US09067905B2

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