Ethyl 3-iodo-2,4-dimethoxy-6-methylbenzoate → Ethyl 6-bromomethyl-3-iodo-2,4-dimethoxybenzoate

HRID 2177846노트

반응식

HRID 2177846 반응식
[Br:1]C1C(OC)=C(C(CSC2C=CC=CC=2)=CC=1)C(OCC)=O.[I:23][C:24]1[C:25]([O:38][CH3:39])=[C:26]([C:32]([CH3:37])=[CH:33][C:34]=1[O:35][CH3:36])[C:27]([O:29][CH2:30][CH3:31])=[O:28]>>[Br:1][CH2:37][C:32]1[C:26]([C:27]([O:29][CH2:30][CH3:31])=[O:28])=[C:25]([O:38][CH3:39])[C:24]([I:23])=[C:34]([O:35][CH3:36])[CH:33]=1

참가 물질

3

반응물 2

HCID 10915077Ethyl 3-iodo-2,4-dimethoxy-6-methylbenzoate2회HCID 67107500HCID 67107500, 화합물

생성물 1

HCID 86677124Ethyl 6-bromomethyl-3-iodo-2,4-dimethoxybenzoate

실험 절차

Prepared by proceeding in a similar manner to Intermediate 87, starting from ethyl 3-iodo-2,4-dimethoxy-6-methylbenzoate (Intermediate 203).

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-d9107393aae246eba434eeadb2405c6c
출처 데이터셋
uspto-grants-2015_06
특허 번호
US09067905B2

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