Ethyl 2-(3-vinylphenyl)acetate → Ethyl 2-(3-ethylphenyl)acetate
반응식
[CH:1]([C:3]1[CH:4]=[C:5]([CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:6]=[CH:7][CH:8]=1)=[CH2:2]>C(O)C.[Pd]>[CH2:1]([C:3]1[CH:4]=[C:5]([CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:6]=[CH:7][CH:8]=1)[CH3:2]참가 물질
4
반응 조건
- 온도
- 30 °C
실험 절차
To a solution of ethyl 2-(3-vinylphenyl)acetate (640 mg, 3.6 mmol) in ethanol (10 mL) was added 10% of Pd/C (100 mg) and stirred at 30° C. under hydrogen atmosphere (15 psi) for 7 hours. Then the solution was filtered and the solvent was removed in vacuo (500 mg, yield 77%).
후처리
- filtrationThen the solution was filtered
- customthe solvent was removed in vacuo (500 mg, yield 77%)
출처 및 근거
- ORD 기록
- ord-6005ba9a255d4059ac2b01de347e9246
- 출처 데이터셋
- uspto-grants-2015_06
- 특허 번호
- US09067893B2
반응 노트
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