Hydrazine → N-(3-Aminopropyl)morpholine

HRID 21785

반응식

HRID 21785 반응식
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][NH2:1])[CH2:4][CH2:5][O:6][CH2:7][CH2:8]1

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 1317183813-Morpholinylpropylphthalimide

생성물 1

HCID 61055N-(3-Aminopropyl)morpholine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 3-morpholinylpropylphthalimide (219 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

후처리

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

출처 및 근거

ORD 기록
ord-31cf6c6cd592407aaa6aa050e8dff730
출처 데이터셋
uspto-grants-1995_06
특허 번호
US05424451

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