1,7-Dibromoheptane → 7-Bromoheptylphthalimide

HRID 21794

반응식

HRID 21794 반응식
[C:1]1(=[O:11])[NH:5][C:4](=[O:6])[C:3]2=[CH:7][CH:8]=[CH:9][CH:10]=[C:2]12.[K].[Br:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]Br>CN(C)C=O>[Br:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][C:10]1[CH:9]=[CH:8][CH:7]=[C:3]2[C:4]([NH:5][C:1](=[O:11])[C:2]=12)=[O:6]

참가 물질

4

반응물 2

HCID 783091,7-DibromoheptaneHCID 24194345Phthalimide potassium salt

생성물 1

HCID 199334987-Bromoheptylphthalimide

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

Potassium phthalimide (5.4 mmoles) was added to a solution of 1,7-dibromoheptane (4.18 g; 16.2 mmoles) in dimethylformamide (8 ml) and heated to 80° C. approx. under stirring. Reaction times and process as per Example 4.

후처리

  1. temperatureheated to 80° C. approx.
  2. customReaction times and process as per Example 4

출처 및 근거

ORD 기록
ord-07d4a24dbc0e49048109010e810572fa
출처 데이터셋
uspto-grants-1995_06
특허 번호
US05424451

연결된 노트

불러오는 중…