홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Methanesulfonic Acid → HCID 131724851, 화합물

HRID 2179911
노트
인쇄 미리보기

반응식

HRID 2179911 반응식
[CH3:1][S:2]([OH:5])(=[O:4])=[O:3].[CH3:6][N:7]([CH3:29])[CH:8]1[C:22]2=[CH:23][CH:19]([O:20][C:21]2=[O:24])[CH:18]2[CH:14]([O:15][C:16](=[O:26])[CH:17]2[CH3:25])[CH2:13][C:12]2([CH3:27])[CH:10]([O:11]2)[CH:9]1[OH:28]>CC(C)=O>[CH3:1][S:2]([O-:5])(=[O:4])=[O:3].[OH:28][CH:9]1[CH:8]([NH+:7]([CH3:6])[CH3:29])[C:22]2=[CH:23][CH:19]([O:20][C:21]2=[O:24])[CH:18]2[CH:14]([O:15][C:16](=[O:26])[CH:17]2[CH3:25])[CH2:13][C:12]2([CH3:27])[CH:10]1[O:11]2
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 6395Methanesulfonic AcidHCID 86592994HCID 86592994, 화합물

생성물 1

HCID 131724851HCID 131724851, 화합물수율 55.4%

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A solution of methanesulphonic acid (0.1 mmol; 1 ml; 0.1N in acetone) is added to a solution of the compound of Example 5 (0.1 mmol; 34 mg) in acetone (2 ml). The precipitate is filtered, washed with acetone and dried under reduced pressure. 24 mg of the expected product is obtained in the form of a white powder. Melting point: 220° C.

후처리

  • filtrationThe precipitate is filtered
  • washwashed with acetone
  • customdried under reduced pressure
  • 출처 및 근거

    ORD 기록
    ord-b68bc0b6d2554ef7ae374df5794cab9f
    출처 데이터셋
    uspto-grants-2005_05
    DOI
    10.6084/m9.figshare.5104873.v1
    특허 번호
    US06887869B2

    반응 노트

    불러오는 중…

    이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트