Hydrazine → HCID 54275604, 화합물

HRID 21807노트

반응식

HRID 21807 반응식
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13][NH2:1]

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 538263884-(N-methylpiperazinyl)butylphthalimide

생성물 1

HCID 54275604HCID 54275604, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-(N-methylpiperazinyl)butylphthalimide (240 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

후처리

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

출처 및 근거

ORD 기록
ord-c944c58f544d4256941c6aa331ac25a9
출처 데이터셋
uspto-grants-1995_06
특허 번호
US05424451

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