Hydrazine → 8-Pyrrolidinyloctylamine

HRID 21813노트

반응식

HRID 21813 반응식
[NH2:1]N.[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7]1

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 542934218-Pyrrolidinyloctylphthalimide

생성물 1

HCID 199335008-Pyrrolidinyloctylamine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-pyrrolidinyloctylphthalimide (263 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

후처리

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

출처 및 근거

ORD 기록
ord-57327deb27424964be85d1a8d0e252d6
출처 데이터셋
uspto-grants-1995_06
특허 번호
US05424451

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