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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2181900생성일: 2026년 10월 24일

Ammonium Acetate → 1-(2',5'-Difluoro-1,1'-biphenyl-2-yl)ethylamine

https://huagongshe.com/ko/reaction/2181900

반응식

참여 물질

역할이름HCID투입량
반응물Ammonium AcetateHCID 517165—
반응물Sodium cyanoborohydrideHCID 5003444—
반응물1-(2',5'-Difluoro-1,1'-biphenyl-2-yl)ethanoneHCID 22482396—
용매MethanolHCID 887—
생성물1-(2',5'-Difluoro-1,1'-biphenyl-2-yl)ethylamineHCID 22482283—

반응 단계

The title compound was prepared from 1-(2′,5′-difluoro-1,1′-biphenyl-2-yl)ethanone (2.0 g, 8.6 mmol), anhydrous methanol (100 mL), ammonium acetate (13.3 g, 172 mmol), and sodium cyanoborohydride (1.08 g, 17.2 mmol) according to the procedure and in the same manner as described in Example 105, step b;

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06894061B2
출처 데이터셋uspto-grants-2005_05
ORD IDord-9465f3c683de4a22b3818456430bdbc4
출처 메모uspto-grants-2005_05