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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2181910생성일: 2026년 10월 26일

Potassium Carbonate → 3,9-Difluoro-5-[(4-methoxyphenyl)sulfonyl]-6-methyl-5,6-dihydrophenanthridine

https://huagongshe.com/reaction/2181910

반응식

참여 물질

역할이름HCID투입량
반응물Potassium CarbonateHCID 11430—
반응물N-[1-(2',4',5-Trifluoro-1,1'-biphenyl-2-yl)ethyl]-4-methoxybenzenesulfonamideHCID 22482340—
용매DimethylformamideHCID 6228—
생성물3,9-Difluoro-5-[(4-methoxyphenyl)sulfonyl]-6-methyl-5,6-dihydrophenanthridineHCID 22482344—

반응 단계

The title compound was prepared from N-[1-(2′,4′,5-trifluoro-1,1′-biphenyl-2-yl)ethyl]-4-methoxybenzenesulfonamide (161 mg, 0.38 mmol), anhydrous N,N-dimethylformamide (1 mL), and potassium carbonate (106 mg, 0.76 mmol) according to the procedure and in the same manner as described in Example 105, step d resulting in the isolation of 143 mg (93%) of a white solid. This material was used without further purification in Example 114, step e;

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06894061B2
출처 데이터셋uspto-grants-2005_05
ORD IDord-8244310883bd41f383daa498fae65b9c
출처 메모uspto-grants-2005_05