Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
[(4-Dimethylaminophenyl)methyl](4-ethylphenyl)amine → N-[(4-dimethylaminophenyl)methyl]-N-(4-ethylphenyl)-6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | [(4-Dimethylaminophenyl)methyl](4-ethylphenyl)amine | HCID 3482181 | — |
| 반응물 | 6,7,8,9-tetrahydro-5H-benzo(7)annulene-5-carboxylic acid | HCID 14822604 | — |
| 생성물 | N-[(4-dimethylaminophenyl)methyl]-N-(4-ethylphenyl)-6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxamide | HCID 10202735 | 19.9% |
반응 단계
By the reaction and treatment in the same manner as in Example 1 using 6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxylic acid (0.54 g) and [(4-dimethylaminophenyl)methyl](4-ethylphenyl)amine (0.6 g) as starting materials, N-[(4-dimethylaminophenyl)methyl]-N-(4-ethylphenyl)-6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxamide (0.2 g) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08198454B2 |
| 출처 데이터셋 | uspto-grants-2012_06 |
| ORD ID | ord-e97a9f9b53c841b6a3c763bd7ce59487 |
| 출처 메모 | uspto-grants-2012_06 |