HCID 597528, 화합물 → HCID 21349890, 화합물

반응식

O[CH2:2][CH2:3][N:4]1[C:9]2[CH:10]=[CH:11][CH:12]=[C:13]([O:14][CH2:15][C:16]([O:18][CH3:19])=[O:17])[C:8]=2[O:7][CH2:6][C:5]1=[O:20].[C:21]1([C:27]([C:30]2[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=2)([SH:29])[CH3:28])[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[C:30]1([C:27]([C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=2)([S:29][CH2:2][CH2:3][N:4]2[C:9]3[CH:10]=[CH:11][CH:12]=[C:13]([O:14][CH2:15][C:16]([O:18][CH3:19])=[O:17])[C:8]=3[O:7][CH2:6][C:5]2=[O:20])[CH3:28])[CH:31]=[CH:32][CH:33]=[CH:34][CH:35]=1

참가 물질

반응물 2

HCID 597528HCID 597528, 화합물

HCID 21349895HCID 21349895, 화합물

생성물 1

HCID 21349890HCID 21349890, 화합물수율 42%

실험 절차

The same process as Example 1 was repeated except that methyl (4-(2-hydroxyethyl)-3-oxo-3,4-dihydro-2H-1,4-benzoxazin-8-yloxy)acetate (187 mg) and 1,1-diphenylethanethiol (270 ml) were used to obtain the object compound (172.5 mg, yield 42%).

출처 및 근거

ORD 기록: ord-917b0c011c764d28949bf971607260f2
출처 데이터셋: uspto-grants-2002_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06407096B1

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