HCID 9803568, 화합물 → HCID 12968239, 화합물

HRID 2187109노트

반응식

HRID 2187109 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:10][C:11]3[CH:31]=[C:30]([O:32][CH3:33])[CH:29]=[CH:28][C:12]=3[C:13]=2[C:14]([C:16]2[CH:21]=[CH:20][C:19]([O:22][CH2:23][CH2:24][N:25]([CH3:27])[CH3:26])=[CH:18][CH:17]=2)=[O:15])=[CH:5][CH:4]=1>CO>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:10][C:11]3[CH:31]=[C:30]([O:32][CH3:33])[CH:29]=[CH:28][C:12]=3[C:13]=2[CH:14]([C:16]2[CH:21]=[CH:20][C:19]([O:22][CH2:23][CH2:24][N:25]([CH3:27])[CH3:26])=[CH:18][CH:17]=2)[OH:15])=[CH:5][CH:4]=1

참가 물질

3

반응물 1

HCID 9803568HCID 9803568, 화합물

생성물 1

HCID 12968239HCID 12968239, 화합물수율 68.5%

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

1.335 g (3 mmol) of [2-(4-methoxyphenyl)-6-methoxybenzofuran-3-yl][4-[2-dimethylaminoethoxy]phenyl]methanone was reduced to the carbinol by the method described in Example 1. This yielded 920 mg of the title compound as an oil.

출처 및 근거

ORD 기록
ord-59160e65c9ee443e8b8bdcf04e44e806
출처 데이터셋
uspto-grants-2002_06
특허 번호
US06407243B1

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