1,1-Dimethyl-2-(3-pyridylmethyl)hydrazine → S-methyl-N-(6-chloro-3-pyridylmethyl)-N-methyl-N'-methylisothiourea

HRID 2187227노트

반응식

HRID 2187227 반응식
[Cl:1][C:2]1[N:7]=[CH:6][C:5]([CH2:8][N:9]([CH3:14])[C:10]([NH:12][CH3:13])=[S:11])=[CH:4][CH:3]=1.[CH3:15]N(C)NCC1C=NC=CC=1.ClC1C(CN)=CC=C(Cl)N=1>>[CH3:15][S:11][C:10](=[N:12][CH3:13])[N:9]([CH2:8][C:5]1[CH:6]=[N:7][C:2]([Cl:1])=[CH:3][CH:4]=1)[CH3:14]

참가 물질

4

반응물 3

HCID 111481501,1-Dimethyl-2-(3-pyridylmethyl)hydrazineHCID 150289211-(6-Chloro-3-pyridylmethyl)-1,3-dimethylthioureaHCID 15477284(2,6-Dichloropyridin-3-YL)methanamine

생성물 1

HCID 22450313S-methyl-N-(6-chloro-3-pyridylmethyl)-N-methyl-N'-methylisothiourea

실험 절차

Using the N-(6-chloro-3-pyridylmethyl)-N-methyl-N′-methylthiourea otained in (1), the procedure of Example 8 (2) was repeated to give S-methyl-N-(6-chloro-3-pyridylmethyl)-N-methyl-N′-methylisothiourea as oil.

출처 및 근거

ORD 기록
ord-7677706e1a6641549de700065d033d24
출처 데이터셋
uspto-grants-2002_06
특허 번호
US06407248B1

반응 노트

불러오는 중…