Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoroacetic acid → 4'-Formylbenzo-15-crown-5
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoroacetic acid | HCID 6422 | — |
| 반응물 | 1,4,7,10,13-Benzopentaoxacyclopentadecin, 2,3,5,6,8,9,11,12-octahydro- | HCID 84197 | — |
| 생성물 | 4'-Formylbenzo-15-crown-5 | HCID 324243 | — |
반응 단계
A solution of hexamethylenetretramine (1.87 mmol, 0.27 g) in trifluoroacetic acid (1.4 cm3) was added to benzo 15-crown-5 ether (1.87 mmol, 0.5 g) under nitrogen; the mixture was heated to reflux for 12 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05425878 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-0aba0da7a8164d719a0f863898cfe358 |
| 출처 메모 | uspto-grants-1995_06 |