N-benzylaminosulfonamide → Benzylsulfamide potassium salt

HRID 2189129노트

반응식

HRID 2189129 반응식
[CH2:1]([NH:8][S:9]([NH2:12])(=[O:11])=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.CC([O-])(C)C.[K+:18]>>[K+:18].[CH2:1]([NH:8][S:9]([NH-:12])(=[O:11])=[O:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

참가 물질

3

반응물 2

HCID 12354987N-benzylaminosulfonamideHCID 23665647Potassium tert-butoxide

생성물 1

HCID 21041359Benzylsulfamide potassium salt수율 100.6%

실험 절차

To a solution of benzylsulfamide (17.98 g) in McOH (300 mL) was carefully added potassium tert-butylate (10.8 g). The mixture was stirred at rt for 15 min before the solvent was evaporated. The remaining residue was dried under HV to give benzylsulfamide potassium salt as an off-white powder (21.73 g).

후처리

  1. customwas evaporated
  2. customThe remaining residue was dried under HV

출처 및 근거

ORD 기록
ord-5d1afc6e2d174f638edd86682471e518
출처 데이터셋
uspto-grants-2012_12
특허 번호
US08324232B2

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