HCID 67312049, 화합물 → HCID 67312567, 화합물

HRID 2190429노트

반응식

HRID 2190429 반응식
[N+:1]([C:4]1[CH:29]=[CH:28][C:7]([O:8][C:9]2[CH:10]=[C:11]([CH:25]=[CH:26][CH:27]=2)[C:12]([NH:14][C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([C:21]([F:24])([F:23])[F:22])[CH:16]=2)=[O:13])=[CH:6][CH:5]=1)([O-])=O>[C].[Pd]>[NH2:1][C:4]1[CH:5]=[CH:6][C:7]([O:8][C:9]2[CH:10]=[C:11]([CH:25]=[CH:26][CH:27]=2)[C:12]([NH:14][C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([C:21]([F:22])([F:23])[F:24])[CH:16]=2)=[O:13])=[CH:28][CH:29]=1

참가 물질

3

반응물 1

HCID 67312049HCID 67312049, 화합물

생성물 1

HCID 67312567HCID 67312567, 화합물수율 69%

시약·촉매·용매 1

HCID 178418390HCID 178418390, 화합물촉매

실험 절차

Using 3-(4-nitrophenoxy)-N-[3-(trifluoromethyl)phenyl]benzamide (2.81 g, 10.0 mmol) and 10%-palladium carbon (1 g), and in the same manner as in Example A25(iv), the title compound (2.45 g, 69%) was obtained as a brown oil.

출처 및 근거

ORD 기록
ord-fa4f97498fa14c3ea70470ea706f3f8b
출처 데이터셋
uspto-grants-2012_12
특허 번호
US08324395B2

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