5-iodo-2,4-dimethyl-1H-imidazole → 5-(4-iodo-2,5-dimethyl-imidazol-1-yl)-2-methyl-2H-pyridazin-3-one

HRID 2194441노트

반응식

HRID 2194441 반응식
Cl[C:2]1[CH:7]=[N:6][N:5]([CH3:8])[C:4](=[O:9])[CH:3]=1.[I:10][C:11]1[N:12]=[C:13]([CH3:17])[NH:14][C:15]=1[CH3:16]>>[I:10][C:11]1[N:12]=[C:13]([CH3:17])[N:14]([C:2]2[CH:7]=[N:6][N:5]([CH3:8])[C:4](=[O:9])[CH:3]=2)[C:15]=1[CH3:16]

참가 물질

3

반응물 2

HCID 6136385-iodo-2,4-dimethyl-1H-imidazoleHCID 129101445-Chloro-2-methylpyridazin-3(2H)-one

생성물 1

HCID 668652885-(4-iodo-2,5-dimethyl-imidazol-1-yl)-2-methyl-2H-pyridazin-3-one

실험 절차

The title compound, light yellow cristalline solid, MS: m/e=331.0 (M+H+), was prepared in accordance with the general method of example 23b from 5-chloro-2-methyl-2H-pyridazin-3-one and 4-iodo-2,5-dimethyl-1H-imidazole.

출처 및 근거

ORD 기록
ord-e1db6c84f8734a94b5233b6defc9cdb8
출처 데이터셋
uspto-grants-2012_12
특허 번호
US08334287B2

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