Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
10-Mercaptomethyl-3-t-butoxycarbonylmethyl-2-oxo-1-azacyclodecane → 10-Mercaptomethyl-2-oxo-1-azacyclodecane-3-acetic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 10-Mercaptomethyl-3-t-butoxycarbonylmethyl-2-oxo-1-azacyclodecane | HCID 19930807 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 10-Mercaptomethyl-2-oxo-1-azacyclodecane-3-acetic acid | HCID 19930854 | — |
반응 단계
10-Mercaptomethyl-3-t-butoxycarbonylmethyl-2-oxo-1-azacyclodecane (0.21 g, 0.69 mmol) is dissolved in methylene chloride (15 mL). Gaseous hydrogen chloride is bubbled through the solvent for 15 minutes, and then the reaction is sealed and stirred overnight. The solvent is evaporated the next day to give 10-mercaptomethyl-2-oxo-1-azacyclodecane-3-acetic acid, MS: M+1=260.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05426103 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-46950eaab8e34cc2a47f6fa0233b2643 |
| 출처 메모 | uspto-grants-1995_06 |