Toluene → Benzene, [2-(1-methylethoxy)ethyl]-

HRID 2198393노트

반응식

HRID 2198393 반응식
C1(C)C=CC=CC=1.C(OC(=O)CC)(=O)CC.C(OC(=O)CC)(=O)CC.C1(C)C=CC=CC=1.C1(CCO)C=CC=CC=1.[CH:42]([O:45][CH2:46][CH2:47][C:48]1[CH:53]=[CH:52][CH:51]=[CH:50][CH:49]=1)([CH3:44])[CH3:43]>O>[CH:42]([O:45][CH2:46][CH2:47][C:48]1[CH:49]=[CH:50][CH:51]=[CH:52][CH:53]=1)([CH3:44])[CH3:43]

참가 물질

5

반응물 3

HCID 1140TolueneHCID 31263Propionic anhydrideHCID 86738357HCID 86738357, 화합물

생성물 1

HCID 106442Benzene, [2-(1-methylethoxy)ethyl]-

시약·촉매·용매 1

HCID 962Water용매

실험 절차

To the toluene mixture is added 260 grams of propionic anhydride and the propionic anhydride/toluene/phenylethyl alcohol/isopropyl phenethylether mixture is then refluxed for a period of 30 minutes. The reaction mass is then cooled down and one liter of water is added thereto. The reaction mass is then washed with 50% caustic followed by saturated sodium chloride and then neutralized with saturated sodium bicarbonate.

후처리

  1. temperatureThe reaction mass is then cooled down
  2. washThe reaction mass is then washed with 50%

출처 및 근거

ORD 기록
ord-2f5405bcef0f4510a4a2dfe37d6215de
출처 데이터셋
uspto-grants-1982_11
특허 번호
US04357319

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