Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Aminoheptane → 1-sec-heptyl-3-n-hexyl-2-S-ethylisothiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Aminoheptane | HCID 5603 | — |
| 반응물 | Iodoethane | HCID 6340 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Hexyl isothiocyanate | HCID 78120 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 1-sec-heptyl-3-n-hexyl-2-S-ethylisothiourea | HCID 13083466 | — |
반응 단계
The equipment, procedure and reactants were the same as in Example 31 with the exception that 10.01 g (0.07 mole) of n-hexylisothiocyanate, 8.05 g (0.07 mole) 2-aminoheptane, 35 ml ethanol 2B, 11.7 g (0.075 mole) ethyl iodide, 200 ml of toluene and a one percent solution sodium hydroxide (0.08 mole) were used as reactants and reagents in the procedure. The reaction produced 19.6 g (98 weight percent of theory yield of a clear liquid having a nD30 of 1.4765. The product was identified as the title product by IR and NMR spectra analyses.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04357351 |
| 출처 데이터셋 | uspto-grants-1982_11 |
| ORD ID | ord-83125b7fc31f4b07bc0367c2d27d4ffe |
| 출처 메모 | uspto-grants-1982_11 |