3-amino-N-ethylpiperidine → 4-amino-N-(1-ethyl-3-piperidyl)benzamide

HRID 2198493

반응식

HRID 2198493 반응식
Cl.[NH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7](Cl)=[O:8])=[CH:5][CH:4]=1.[NH2:12][CH:13]1[CH2:18][CH2:17][CH2:16][N:15]([CH2:19][CH3:20])[CH2:14]1>>[NH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([NH:12][CH:13]2[CH2:18][CH2:17][CH2:16][N:15]([CH2:19][CH3:20])[CH2:14]2)=[O:8])=[CH:5][CH:4]=1

참가 물질

3

반응물 2

HCID 980943-amino-N-ethylpiperidineHCID 186880854-Aminobenzoyl chloride--hydrogen chloride (1/1)

생성물 1

HCID 205201434-amino-N-(1-ethyl-3-piperidyl)benzamide

실험 절차

4-Aminobenzoyl chloride hydrochloride is reacted with 3-amino-1-ethylpiperidine to afford 4-amino-N-(1-ethyl-3-piperidyl)benzamide which is reacted with 4-chloro-8-trifluoromethylquinoline to afford the title compound, melting point 177°-178° C.

출처 및 근거

ORD 기록
ord-a594838f3ce64eb8b8f383b693a5db67
출처 데이터셋
uspto-grants-1982_11
특허 번호
US04357333

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