Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromopropane → HCID 20519071, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromopropane | HCID 6358 | — |
| 반응물 | Cyclododecanemethanol | HCID 74686 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 20519071 | HCID 20519071 | — |
반응 단계
According to the disclosure of Example 1, 99 g of hydroxymethylcyclododecane was first converted into the sodium alcoholate. 74 g (0.6 mol) of 2-bromopropane was added dropwise to the boiling suspension, and then the mixture was heated for 30 hours under reflux. The reaction mixture was poured into water, the organic phase was washed with water, dried over Na2SO4, and then distilled.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04359588 |
| 출처 데이터셋 | uspto-grants-1982_11 |
| ORD ID | ord-dcbf17b5baba4e33805706cfee481f0a |
| 출처 메모 | uspto-grants-1982_11 |