2-Bromopropane → HCID 20519071, 화합물

HRID 2198798

반응식

HRID 2198798 반응식
[OH:1][CH2:2][CH:3]1[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.Br[CH:16]([CH3:18])[CH3:17]>O>[CH:3]1([CH2:2][O:1][CH:16]([CH3:18])[CH3:17])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]1

참가 물질

4

반응물 2

HCID 63582-BromopropaneHCID 74686Cyclododecanemethanol

생성물 1

HCID 20519071HCID 20519071, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

According to the disclosure of Example 1, 99 g of hydroxymethylcyclododecane was first converted into the sodium alcoholate. 74 g (0.6 mol) of 2-bromopropane was added dropwise to the boiling suspension, and then the mixture was heated for 30 hours under reflux. The reaction mixture was poured into water, the organic phase was washed with water, dried over Na2SO4, and then distilled.

후처리

  1. temperaturethe mixture was heated for 30 hours
  2. temperatureunder reflux
  3. washthe organic phase was washed with water
  4. dry with materialdried over Na2SO4
  5. distillationdistilled

출처 및 근거

ORD 기록
ord-dcbf17b5baba4e33805706cfee481f0a
출처 데이터셋
uspto-grants-1982_11
특허 번호
US04359588

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