참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Isopropylamine | HCID 6363 | — |
| 반응물 | (((1,3-Dibromopropan-2-yl)oxy)methyl)benzene | HCID 561824 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1-(Iso-propyl)-3-benzyloxyazetidine | HCID 20517324 | — |
반응 단계
11 Parts of 2-benzyloxy-1,3-dibromo-propane, 30 parts of iso-propylamine and 30 parts of water were added to a stainless autoclave, and the mixture was heated at 80° C. for 2 hours with agitation. The reaction mixture was cooled and treated in the same manner as in Example 29, followed by distillation under reduced pressure. As a result, 18 parts of 3-benzyloxy-1-(iso-propyl)azetidine boiling at 104°-107° C. under 2 mm Hg were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04360464 |
|---|
| 출처 데이터셋 | uspto-grants-1982_11 |
|---|
| ORD ID | ord-254474e6da6d4692a5dc96eee36f2060 |
|---|
| 출처 메모 | uspto-grants-1982_11 |
|---|
