Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 5-bromopyridine-3-carboxylate → Methyl 5-(4-ethylphenyl)pyridine-3-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 5-bromopyridine-3-carboxylate | HCID 699336 | — |
| 반응물 | Boronic acid, (4-ethylphenyl)- | HCID 2734352 | — |
| 생성물 | Methyl 5-(4-ethylphenyl)pyridine-3-carboxylate | HCID 58002322 | — |
반응 단계
According to General Method 3A, 32 g (148 mmol) of methyl 5-bromonicotinate and 27 g (178 mmol, 1.2 eq.) of 4-ethylphenylboronic acid were reacted. Yield: 24 g (64% of theory)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08202862B2 |
| 출처 데이터셋 | uspto-grants-2012_06 |
| ORD ID | ord-b6e49e33a74f4231b8f1b4a940e0c780 |
| 출처 메모 | uspto-grants-2012_06 |