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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 220227생성일: 2026년 10월 25일

Triethylene glycol monomethyl ether → Cyclopropanecarboxylic Acid, 2-[2-(2-Methoxy-ethoxy)-ethoxy]-ethyl Ester

https://huagongshe.com/reaction/220227

반응식

참여 물질

역할이름HCID투입량
반응물Triethylene glycol monomethyl etherHCID 8178—
반응물TriethylamineHCID 8471—
반응물Cyclopropanecarbonyl chlorideHCID 77637—
용매DichloromethaneHCID 6344—
생성물Cyclopropanecarboxylic Acid, 2-[2-(2-Methoxy-ethoxy)-ethoxy]-ethyl EsterHCID 10149156—

반응 조건

온도0 °C

반응 단계

Triethylene glycol monomethyl ether (1.1 eq, 5.26 mmol, 0.84 ml) and triethylamine (1.1 eq, 5.26 mmol, 0.73 ml) were taken in a 10 ml round bottom flask and dichloromethane (3 ml) was added. This mixture was cooled to 0° C. and then cyclopropanecarbonyl chloride (4.78 mmol, 0.5 g, 0.43 ml) was added in a dropwise fashion maintaining the temperature at 0° C. with constant stirring.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08202901B2
출처 데이터셋uspto-grants-2012_06
ORD IDord-8036ff2e445744e1b3e246348875f82e
출처 메모uspto-grants-2012_06