Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 220227생성일: 2026년 10월 25일
Triethylene glycol monomethyl ether → Cyclopropanecarboxylic Acid, 2-[2-(2-Methoxy-ethoxy)-ethoxy]-ethyl Ester
https://huagongshe.com/reaction/220227
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triethylene glycol monomethyl ether | HCID 8178 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Cyclopropanecarboxylic Acid, 2-[2-(2-Methoxy-ethoxy)-ethoxy]-ethyl Ester | HCID 10149156 | — |
반응 단계
Triethylene glycol monomethyl ether (1.1 eq, 5.26 mmol, 0.84 ml) and triethylamine (1.1 eq, 5.26 mmol, 0.73 ml) were taken in a 10 ml round bottom flask and dichloromethane (3 ml) was added. This mixture was cooled to 0° C. and then cyclopropanecarbonyl chloride (4.78 mmol, 0.5 g, 0.43 ml) was added in a dropwise fashion maintaining the temperature at 0° C. with constant stirring.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08202901B2 |
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| 출처 데이터셋 | uspto-grants-2012_06 |
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| ORD ID | ord-8036ff2e445744e1b3e246348875f82e |
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| 출처 메모 | uspto-grants-2012_06 |
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