Isobutyl iodide → HCID 118251639, 화합물

반응식

[CH3:1][O:2][C:3]([C:5]1[CH:6]=[C:7]([Br:14])[CH:8]=[C:9]2[C:13]=1[NH:12][N:11]=[CH:10]2)=[O:4].I[CH2:16][CH:17]([CH3:19])[CH3:18]>>[CH3:1][O:2][C:3]([C:5]1[CH:6]=[C:7]([Br:14])[CH:8]=[C:9]2[C:13]=1[N:12]([CH2:16][CH:17]([CH3:19])[CH3:18])[N:11]=[CH:10]2)=[O:4]

참가 물질

반응물 2

HCID 10556Isobutyl iodide

HCID 24728927Methyl 5-bromo-1H-indazole-7-carboxylate

생성물 1

HCID 118251639HCID 118251639, 화합물수율 70%

실험 절차

Compound 10 was prepared following general method 1, using 5-bromo-1H-indazole-7-carboxylic acid methyl ester as starting material and 1-iodo-2-methylpropane as alkylating agent. Yield: 70%.

출처 및 근거

ORD 기록: ord-a25b0e820bf04ed79002f6b8f142ed2b
출처 데이터셋: uspto-grants-2016_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09365569B2

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