Isopropyl iodide → HCID 118251657, 화합물

반응식

[CH3:1][O:2][C:3]([C:5]1[CH:6]=[C:7]([Br:14])[CH:8]=[C:9]2[C:13]=1[NH:12][N:11]=[CH:10]2)=[O:4].I[CH:16]([CH3:18])[CH3:17]>>[CH3:1][O:2][C:3]([C:5]1[CH:6]=[C:7]([Br:14])[CH:8]=[C:9]2[C:13]=1[N:12]([CH:16]([CH3:18])[CH3:17])[N:11]=[CH:10]2)=[O:4]

참가 물질

반응물 2

HCID 6362Isopropyl iodide

HCID 24728927Methyl 5-bromo-1H-indazole-7-carboxylate

생성물 1

HCID 118251657HCID 118251657, 화합물수율 65%

실험 절차

Compound 14 was prepared following general method 1, using 5-bromo-1H-indazole-7-carboxylic acid methyl ester as a starting material and 2-iodopropane as alkylating agent. Yield: 65%.

출처 및 근거

ORD 기록: ord-e62e5e39766143ecbf261cd30c2b56ba
출처 데이터셋: uspto-grants-2016_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09365569B2

반응 노트

불러오는 중…