Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → N-(4-Fluoro-2-methylphenyl)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| 생성물 | N-(4-Fluoro-2-methylphenyl)acetamide | HCID 2737623 | 74% |
반응 단계
A mixture of 4-fluoro-2-methylaniline (20 g) and (CH3CO)2O (400 mL) was stirred at RT for 3 hours. The reaction mixture was subsequently poured into ice water (1000 mL), stirred for 10 minutes, filtered, and dried under vacuum to give the title compound (20 g, 74%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09365566B2 |
| 출처 데이터셋 | uspto-grants-2016_06 |
| ORD ID | ord-259c4edab98645ea991b35ce6b268676 |
| 출처 메모 | uspto-grants-2016_06 |