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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2205252생성일: 2026년 10월 27일

1,2-Dichloroethane → 1-(2-(2,3-Dimethylbut-2-en-1-yl)indolin-1-yl)ethanone

https://huagongshe.com/reaction/2205252

반응식

참여 물질

역할이름HCID투입량
반응물1,2-DichloroethaneHCID 11—
반응물IndoleHCID 798—
반응물Tin tetrachlorideHCID 24287—
반응물3H-IndoleHCID 3083560—
반응물3,3,4-Trimethylpent-4-en-2-oneHCID 13262537—
생성물1-(2-(2,3-Dimethylbut-2-en-1-yl)indolin-1-yl)ethanoneHCID 7152587958%

반응 단계

Following the general procedure as described in Example 11, 3,3,4-trimethylpent-4-en-2-one (0.50 g, 3.96 mmol), 1H-indole (0.56 g, 4.75 mmol) which was in situ isomerized to 3H-indole, and SnCl4 (1.24 g, 4.75 mmol) in 1,2-dichloroethane (40 ml) were reacted to give the title product as a white solid (0.56 g, 58%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09371262B2
출처 데이터셋uspto-grants-2016_06
ORD IDord-cfeb19e361a74c21b17c8dd50fedbe70
출처 메모uspto-grants-2016_06