2-(Methylsulfonyl)ethanol → HCID 86717279, 화합물

HRID 2205781노트

반응식

HRID 2205781 반응식
[Cl:1][C:2]1[C:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[N:6][N:5]=[C:4]2[NH:14][N:15]=[C:16]([CH:17]3[CH2:19][CH2:18]3)[C:3]=12.[CH3:20][S:21]([CH2:24][CH2:25]O)(=[O:23])=[O:22]>>[Cl:1][C:2]1[C:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[N:6][N:5]=[C:4]2[N:14]([CH2:25][CH2:24][S:21]([CH3:20])(=[O:23])=[O:22])[N:15]=[C:16]([CH:17]3[CH2:19][CH2:18]3)[C:3]=12

참가 물질

3

반응물 2

HCID 848342-(Methylsulfonyl)ethanolHCID 86717280HCID 86717280, 화합물

생성물 1

HCID 86717279HCID 86717279, 화합물

실험 절차

Compound Ix was synthesized from 4-chloro-3-cyclopropyl-5-phenyl-1H-pyrazolo[3,4-c]pyridazine and 2-(methylsulfonyl)ethanol following the general procedure for the Mitsunobu reaction as described above.

후처리

  1. customfor the Mitsunobu reaction

출처 및 근거

ORD 기록
ord-5eef986ef3c1468086b12dce5be62e08
출처 데이터셋
uspto-grants-2016_06
특허 번호
US09371332B2

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