Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen chloride-ethyl acetate → Oxan-4-ylhydrazine dihydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| 반응물 | N'-(oxan-4-yl)(tert-butoxy)carbohydrazide | HCID 45092245 | — |
| 생성물 | Oxan-4-ylhydrazine dihydrochloride | HCID 50988431 | — |
반응 단계
tert-Butyl 2-(tetrahydro-2H-pyran-4-yl)hydrazinecarboxylate (1.82 g) was dissolved in 4N hydrogen chloride-ethyl acetate solution (85 mL) under ice-cooling, and the solution was stirred overnight at room temperature. The reaction mixture was concentrated under reduced pressure to give the title compound (1.52 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09371320B2 |
| 출처 데이터셋 | uspto-grants-2016_06 |
| ORD ID | ord-e0bf9401af274c7fb0f43c5a4cd2ab76 |
| 출처 메모 | uspto-grants-2016_06 |