Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pentanamide → N,N'-((4-(diethylamino)phenyl)methylene)dipentanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pentanamide | HCID 12298 | — |
| 반응물 | 4-(Diethylamino)benzaldehyde | HCID 67114 | — |
| 생성물 | N,N'-((4-(diethylamino)phenyl)methylene)dipentanamide | HCID 71451973 | 69% |
반응 단계
Compound 52 was prepared from pentanamide and 4-(diethylamino)benzaldehyde using method 1. Yield: 69%. 1H NMR (400 MHz, CD3OD) δ 7.18 (d, J=8.8 Hz, 2H), 6.71 (d, J=8.8 Hz, 2H), 6.58 (t, J=8.4 Hz, 1H), 3.33-3.41 (m, 4H), 2.25 (t, J=7.2 Hz, 4H), 1.58-1.66 (m, 4H), 1.33-1.43 (m, 4H), 1.14 (t, J=7.2 Hz, 6H), 0.95 (t, J=2.8 Hz, 6H). LC-MS (ESI): m/z 362.2 (M+H)+. HRMS (ESI) for C21H36N3O2 (MH+): calcd, 362.2802. found 362.2792.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09376380B2 |
| 출처 데이터셋 | uspto-grants-2016_06 |
| ORD ID | ord-2749e43e622e4e3bb4738f309f0173bd |
| 출처 메모 | uspto-grants-2016_06 |