Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Diethylamino)benzaldehyde → N,N'-((4-(diethylamino)phenyl)methylene)dioctanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Diethylamino)benzaldehyde | HCID 67114 | — |
| 반응물 | Octanamide | HCID 69414 | — |
| 생성물 | N,N'-((4-(diethylamino)phenyl)methylene)dioctanamide | HCID 71453778 | 68% |
반응 단계
Compound 54 was prepared from octanamide and 4-(diethylamino)benzaldehyde using method 1. Yield: 68%. 1H NMR (400 MHz, DMSO) δ 8.21 (d, J=8.0 Hz, 2H), 7.07 (d, J=8.8 Hz, 2H), 6.61 (d, J=8.8 Hz, 2H), 6.42 (t, J=8.0 Hz, 1H), 3.29-3.31 (m, 4H), 2.06-2.14 (m, 4H), 1.47-1.50 (m, 4H), 1.08-1.24 (m, 16H), 1.06 (t, J=7.2 Hz, 6H), 0.94 (t, J=7.2 Hz, 6H). LC-MS (ESI): m/z 446.3 (M+H)+. HRMS (ESI) for C27H48N3O2 (MH+): calcd, 446.3741. found 446.3734.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09376380B2 |
| 출처 데이터셋 | uspto-grants-2016_06 |
| ORD ID | ord-642ddc2f691b410294d80999453880e4 |
| 출처 메모 | uspto-grants-2016_06 |